Synthesis of new phenanthro imidazole derivatives in solvent free condition
الموضوعات : International Journal of Heterocyclic Chemistry
1 - Department of Chemistry, Science and Research Branch, Islamic Azad University, Tehran, Iran
الکلمات المفتاحية: Microwave, One-pot, Multicomponent reaction, Imidazoles,
ملخص المقالة :
phenanthro Imidazole derivatives were made synthesis the combinations of phenanthroquinone , Benzealdehyde derivatives in the presence of amines compounds. In all reactions, reactions were investigated under Microwave conditions. The structure of all compounds was studied by an IR Spectrums and 1HNMR Spectrums. Excellent yields, short reaction times, simplicity of operation and easy separation are several advantages of this technique. The results shown that the optimal conditions for the formation of phenanthro derivative of imidazole are at 70 ˚C, the power of 400 W and the time of two minutes.