سنتز سبز نانوذرات نقره با استفاده از عصاره آبی بذر بادیان رومی (Pimpinella anisum) و بررسی فعالیت آنتی اکسیدانی آن
الموضوعات :
علی سرداریان
1
,
وحید حکیم زاده
2
,
سید هاشم اخلاقی فیض اباد
3
1 - دانشگاه آزاد اسلامی واحد قوچان
2 - استاد یار گروه علوم صنایع غذایی دانشگاه آزاد اسلامی واحد قوچان
3 - دانشیار گروه شیمی دانشگاه آزاد اسلامی واحد سبزوار
الکلمات المفتاحية: XRD, SEM, Pimpinella anisum, نانوذرات نقره, جسم کریستالی (متبلور),
ملخص المقالة :
Pimpinella anisum، گیاه دارویی یک ساله و متعلق به خانواده Apiaceae است. این گونه به صورت گسترده پخش شده و در اروپا، ترکیه، ایران قفقاز، آسیای مرکزی، سوریه و مصر یافت میشود عصاره مایع Pimpinella anisum برای سنتز سبز نانوذرات نقره با استفاده از احیاء زیستی محلول مایع نیترات نقره استفاده گردید. خواص نانو ذرات نقره به وسیله طیف سنجی UV-Vis، تبدیل فوریه طیف سنجی مادون قرمز (FTIR)، آنالیز انکسار اشعه X (XRD)، اسکن میکروسکوپ الکترونی (SEM) و آنالیز پراکنش انرژی اشعه X (EDAX) تعیین گردید. افزایش میزان جذب در طول موج 420 nm برای ثبت تشکیل یک سوسپانسیون کلوئیدی از نانوذرات نقره استفاده شد. خصوصیات اتصال نانوذرات نقره اندود سنتز شده از عصاره مایع Pimpinella anisum به وسیله FTIR آنالیز شدند. مطالعات XRD نشان دادند که بسیاری از نانوذرات مکعبی بوده و سیمایی مکعب محور از نظر شکل داشتند. آنالیز SEM، اندازه و شکل نانوذرات نقره را نشان داد و EDAX حضور نقره را تایید کرد. نانوذرات سنتز شده نقره، فعالیت مهار رادیکالهای آزاد DPPH را نشان دادند.
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