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مقاله
1 - A Highly Efficient Protocol for the Synthesis of 2-Amidoalkylphenols using SO3H-Functionalized Phthalimide (SFP) under Solvent-free ConditionsJournal of Applied Chemical Research , شماره 4 , سال 10 , تابستان 2016A highly efficient and simple protocol for the synthesis of 2-amidoalkylphenols has been described. The one-pot multi-component condensation of phenols with aromatic aldehydes and amides in the presence of catalytic amount of SO3H-functionalized phthalimide (SFP) under چکیده کاملA highly efficient and simple protocol for the synthesis of 2-amidoalkylphenols has been described. The one-pot multi-component condensation of phenols with aromatic aldehydes and amides in the presence of catalytic amount of SO3H-functionalized phthalimide (SFP) under solvent-free conditions afford the title compounds in high yields and relatively short reaction times. It is noteworthy that the reaction between phenols, arylaldehydes and amides has been scarcely studied in the literature (in spite of the condensation of 2-naphthol with arylaldehydes and amides, which has been extensively reported). پرونده مقاله -
مقاله
2 - Synthesis and Identification of SO3H-functionalized Phthalimide (SFP) as an Efficient Catalyst for the Condensation of Dimedone with ArylaldehydesAbdolkarim Zare Hakimeh Asvar Fatemeh Zarei Maryam Khalili Zahra Kordrostami Ahmad Reza Moosavi-Zare Vahid KhakyzadehJournal of Applied Chemical Research , شماره 2 , سال 10 , بهار 2016A SO3 H-containing solid acid namely SO3 H-functionalized phthalimide (SFP) was synthesized from phthalimide and chlorosulfonic acid, and identified by studying its FT-IR, 1 H and 13C NMR, Mass, XRD, TG and DTG spectra. Afterward, its catalytic activity was examined for چکیده کاملA SO3 H-containing solid acid namely SO3 H-functionalized phthalimide (SFP) was synthesized from phthalimide and chlorosulfonic acid, and identified by studying its FT-IR, 1 H and 13C NMR, Mass, XRD, TG and DTG spectra. Afterward, its catalytic activity was examined for the solvent-free condensation of dimedone (5,5-dimethyl-1,3-cyclohexanedione) (2 eq.) with arylaldehydes (1 eq.). The results showed that SFP is a highly efficient catalyst to promote the title reaction for the preparation of 9-aryl-1,8-dioxo-octahydroxanthenes. پرونده مقاله