Copper manganese ferrite nanoparticles production via co precipitation method and study of its sensitivity property for ethanol detection

Subject Areas :

Hamid Reza  Ebrahimi ¹ (عضو هیات علمی)
Majid  Mozaffari ² (عضو هیات علمی)
Hasan  Ghafuri Varzaneh ³ (عضو هیات علمی)
Syed Alireza  Sorori ⁴ (Faculty)

Received: 2016-04-22 Accepted : 2018-02-19 Published : 2018-02-20

Keywords: ethanol, X-ray diffraction, Sensitivity, Copper manganese ferrite nanoparticles,

Abstract :

A copper manganese ferrite nanoparticles from effective ferrites that applicable in sensitivity investigations was prepared in this study. Co-precipitation method was used for synthesis of this ferrite that is useful method for synthesizing of these compounds. For structure evaluation, X-ray diffraction (XRD) experiments for phase formation confidence and transmission electron microscopy (TEM) for formation of nanoparticles below 30 nm scale confidence were used. By X-ray fluorescence (XRF) experiment exact percent of each element was determined in copper manganese ferrite compound. By (AGFM) experiments the magnetic behavior of powder and disk sample of copper manganese ferrite nanoparticles was determined. For sensitivity properties investigation of these nanoparticles, mentioned nanoparticles were converted to a tablet form. This tablet was putted in a temperature controlled box. Nine solvents were vaporized (gases) and exposed to this nanoparticles. Responses to these gases were transmitted to a computer by an electronic board connection. Result information was analyzed by software. Sensitivity study of this nano sensor was tested by using carbon tetrachloride, ethanol, methanol, acetonitrile, acetone, vinyl acetate, acrylonitrile, ammonia and formamide. Among these gases ethanol had the best sensitivity in 100˚C temperature.

References:

 [1]    A. D. Wilson & M. Baietto, “Applications and Advances in Electronic-Nose Technologies”, sensors, Vol. 9, pp. 50, 2009.

 

[2]    F. Toshio, “Keynote speaker I: Cell analysis and assembly by micro and nano robotics system”, in Region 10 Symposium, Vol. 10, pp. 1-5, 2014.

 

[3]    S. Ayşin & M. Ezel, “Nanotechnology Innovations for the Sustainable Buildings of the Future”, Architectural and Environmental Engineering, Vol. 8, pp. 1, 2014.

 

[4]    R. D. Ladhe, K. V. Gurav, S. M. Pawar, J. H. Kim & B. R. Sankapal, “p-PEDOT: PSS as a heterojunction partner with n-ZnO for detection of LPG at room temperature”, Journal of Alloys and Compounds, Vol. 5015, pp. 80-85, 2012.

 

[5]    M. M. Rahman, G. Gruner, M. S. Al-Ghamdi, M. S. Daous, S. Bahadar Khan & A. M. Asiri, “Chemo-sensors development based on low-dimensional codoped Mn2O3-ZnO nanoparticles using flat-silver electrodes”, Chemistry Central Journal, Vol. 1, pp. 7-60, 2013.

 

[6]    S. Singh, N. Verma, B. C. Yadav & R. Prakash, “A comparative study on surface morphological investigations of ferric oxide for LPG and opto-electronic humidity sensors”, Surface Science, Vol. 258, pp. 8780-8789, 2012.

 

[7]    B. C. Yadav, S. Singh & A. Yadav, “Nanonails structured ferric oxide thick film as room temperature liquefied petroleum gas (LPG) sensor”, Surface Science,Vol. 257, pp. 1960-1966, 2011.

 

[8]    K. Winiarska, I. Szczygieł & R. Klimkiewicz, “Manganese–Zinc Ferrite Synthesis by the Sol–Gel Autocombustion Method. Effect of the Precursor on the Ferrite’s Catalytic Properties”, American Chemical Society, Vol. 52, No. 1, pp. 353-361, 2013.

 

[9]    R. B. Kamble & V. L. Mathe, “Nanocrystalline nickel ferrite thick film as an efficient gas sensor at room temperature”, Sensors and Actuators, Vol. 131B, pp. 205-209, 2008.

 

[10] S. Zhipeng, L. Lang, J. Dian zeng & P. Weiyu, “Simple synthesis of CuFe2O4 nanoparticles as gas-sensing materials”, Sensors and Actuators, Vol. 125B, pp. 144-148, 2007.

 

[11] S. S. Joshi, C. D. Lokhande & H. H. Sung, “A room temperature liquefied petroleum gas sensor based on all-electrodeposited n-CdSe/p-polyaniline junction”, Sensors and Actuators, Vol. 123B, pp. 240-245, 2007.

 

[12] I. Polaert, S. Bastien, B. Legras, L. Estel & N. Braidy, “Dielectric and magnetic properties of NiFe2O4 at 2.45 GHz and heating capacity for potential uses under microwaves”, Journal of Magnetism and Magnetic Materials, pp. 731-739, 2015.

 

[13] H. Meixner, J. Wiley & Sons, “Micro-and Nanosensor Technology: Trends in Sensor Markets”, Sensors, No. 8, pp. 1, 2008.

 

[14] M. K. Jaiswal, D. Mrinmoy, S. S. Chou, S. Vasavada, R. Bleher, P. V. Prasad, D. Bahadur & V. P. Dravid, “Thermoresponsive Magnetic Hydrogels as Theranostic Nanoconstructs”, American Chemical Society, Vol. 6, pp. 6237-6247, 2014.

 

[15] S. Balasubramaniam, S. Kayandan, Y. N. Lin, D. F. Kelly, W. C. Robert, S. G. Timothy & M. J. House, “Toward Design of Magnetic Nanoparticle Clusters Stabilized by Biocompatible Diblock Copolymers for T2-Weighted MRI Contrast”, American Chemical Society, Vol. 30, No. 6, pp. 1580-1587, 2014.

 

[16] R. V. Roosbroeck, W. V. Roy, T. Stakenb, J. Trekker, A. D. Hollander, T. Dresselaer, J. Lammertyn & L. Lagae, “Synthetic Antiferromagnetic Nanoparticles as Potential Contrast Agents in MRI”, American Chemical Society, Vol. 8, pp. 2269-2278, 2014.

 

[17] M. K. Jaiswal, M. De, S. S. Chou, S. Vasavada, R. Bleher, P. V. Prasad, D. Bahadur & V. P. Dravid., “Thermoresponsive Magnetic Hydrogels as Theranostic Nanoconstructs”, American Chemical Society,Vol. 6, No. 9, pp. 6237-6247, 2014.

 

[18] R. Sharma, A. Sharma & C. J. Chen, “State of Art on Bioimaging by Nanoparticles in Hyperthermia and Thermometry: Visualization of Tissue Protein Targeting”, The Open Nanomedicine Journal, Vol. 3, pp. 10-23, , 2011.

 

[19] F. Morrison, A. Becker, U. Conti & E. Gasperikova, “Ferrite-Cored Solenoidal Induction Coil Sensor For Bud (MM-1667) ”, Lawrence Berkeley National Laboratory, Vol. 26, pp. 1667, 2011.

 

[20] E. S. Zohora, A. M. Khan, A. K. Srivastava & N. Hundewale, “Chemical Sensors Employed In Electronic Noses”, International Journal of Soft Computing and Engineering (IJSCE), Vol. 2, pp. 405-408, 2013.

 

[21] R. Shakya, K. Rajanwal & S. Patel, “Comparative Analysis of Fuzzy Logic Controller and Conventional PID for Temperature Control”, International Journal of Advances in Engineering Science and Technology, Vol. 383, pp. 383-389, 2013.

 

[22] K. S. Mousavi Mashhadi, M. Zahiri Savzevar & J. Ghobadi Dizaj Yekan, “Simulation of Temperature Controller for an Injection Mould Machine using Fuzzy Logic”, Journal of mathematics and computer Science, Vol. 7, pp. 33-42, 2013.

 

[23] C. Brandt, “The Identification of Chemicals using Clustering and Extrapolation From an External Database for Electronic Nose Sensors”, Journal of Young Investigators, Vol. 1, pp. 5, 2008.

 

C. Brandt, “The Identification of Chemicals using Clustering and Extrapolation From an External Database for Electronic Nose Sensors”, Journal of Young Investigators, Vol. 1, pp. 5, 2008.