Biosynthesis and characterization of silver nanoparticles using aqueous extract of walnut (Juglans regia L.) leaf
Subject Areas :masoud bayat 1 , reza moradi 2 , ali bodaghi 3
1 - Department of Chemistry, Tuyserkan Branch, Islamic Azad University, Tuyserkan, Iran
2 - Department of Chemistry, Tuyserkan Branch, Islamic Azad University, Tuyserkan, Iran
3 - Department of Chemistry, Tuyserkan Branch, Islamic Azad University, Tuyserkan, Iran
Keywords: silver nanoparticles, Extract, Walnut leaf, biosynthesis, Surface plasmon resonance,
Abstract :
Green synthesis of nanoparticles is an environmentally friendly method, in which water solvent are used. In this study, the biosynthesis of silver nanoparticles (Ag-NPs) was performed by using walnut (Juglans regia L.) leaf extract. Walnut leaf contains a variety of chemicals, including tannins, flavonoids, vitamins, plant acids and naphthoquinone. The extract of walnut (Juglans regia L.) leaf as the reducing agent is used for the synthesis of silver nanoparticles. The silver nanoparticles have been characterized by scanning electron microscopy (SEM), Energy dispersive X-ray (EDAX), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR) and UV-Visible spectroscopy. UV-Vis spectrum exhibit an absorption band at around 400-450 nm suggestion the formation of silver nanoparticles. The observed peak at about 425 nm is related to the surface plasmon resonance of silver nanoparticles. The effects of operational parameters in the synthesis of silver nanoparticles such as silver nitrate salt concentration, extract volume, temperature and time was studied. The results showed that silver nitrate concentration 6 mM, extract volume 200 µlit, temperature 90°C and time 40 min was the optimum amounts.
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[1] Mishra, M.; Chauhan, P.; J. Nanomed. Res. 2, 1-10, 2015.
[2] Bi, S.S.; Shi, L.; Zhang, L.L.; Applied Thermal Eng. 28, 1834-1843, 2008.
[3] Gad-Allah, T.A.; Kato, S.; Satokawa, S.; Kojima, T.; Desalination 244, 1-11, 2009.
[4] Swihart, M.T.; Current Opinion in Colloid & Interface Science 8, 127-133, 2003.
[5] Sharma, V.K.; Yngard, R.A.; Lin, Y.; Advances in colloid and interface science. 145, 83-96, 2009.
[6] Waksmundzka-Hajnos, M.; Sherma, J.; Kowalska, T.; “Thin layer chromatography in phytochemistry”, CRC Press, Boca Raton, 2008.
[7] Bruneton, J.P.; “Phytochimie. Plantes médicinales”, 2nd ed., Lavoisier, Paris, 1993.
[8] Zargari, A.; “Medicinal plants”, 4th Edition, University of Tehran Press, Iran, 1990.
[9] Pereira, J.A.; Oliveira, I.; Sousa, A.; Valentão, P.; Andrade, P.B.; Ferreira, I.C.; Estevinho, L.; Food and Chemical Toxicology 45, 2287-2295, 2007.
[10] Chaleshtori, R.S.; Chaleshtori, F.S.; Rafieian, M.; Turkish Journal of Biology 35, 635-639, 2011.
[11] Tamasa, P.; Suman, J.; “Synthesis and Characterization of Silver Nanoparticles Using Leaf Extract of Azadirachta indica”, Rourkela, India, 2013.
[12] Roy, N.; Barik, A.; International Journal of Nanotechnology and applications. 4, 95-101, 2010.
[13] Sreemanti, D.; Jayeeta, D.; Asmita, S.; Soumya Sundar, B.C.; Durba, D.; Anisur, R.; Khuda, B.; Colloids Surf. B: Biointerfaces 101, 325 -336, 2013.
[14] Rai, A.; Singh, A.; Ahmad, A.; Sastry, M.; Langmuir 22, 736-741, 2006.
[15] Hussain, I.; Singh, N.B.; Singh, A.; Singh, H.; Singh, S.C.; Biotechnology Letters 38, 545-560, 2016.
[16] Shahverdi, A.R.; Minaeian, S.; Shahverdi, H.R.; Jamalifar, H.; Nohi, A.A.; Process Biochemistry 42, 919-923, 2007.
[17] Darvishi, E.; Kahrizi, D.; Arkan, E.; Journal of Molecular Liquids 286, 110831, 2019.
[18] Sellmann, D.; Nakamoto, K.; “Infrared Spectra of Inorganic and Coordination Compounds”, John Wiley & Sons, New York, 1971.
[19] Izadiyan, Z.; Shameli, K.; Miyake, M.; Hara, H.; Mohamad, S.E.B.; Kalantari, K.; Taib, S.H.M.; Rasouli, E.; Arabian Journal of Chemistry 13, 2011-2023, 2020.
[20] Seifipour, R.; Nozari, M.; Pishkar, L.; Journal of Inorganic and Organometallic Polymers and Materials 30, 2926-2936, 2020.
[21] Jebril, S.; Khanfir Ben Jenana, R.; Dridi, Ch.; Materials Chemistry and Physics 248, 122898, 2020.
[22] Dwivedi, A.D.; Gopal, K.; Colloids and Surfaces A: Physicochemical and Engineering Aspects 369, 27-33, 2010.
[23] Dubey, S.P.; Lahtinen, M.; Sillanpää, M.; Process Biochemistry 45, 1065-1071, 2010.
[24] Piñero, S.; Camero, S.; Blanco, S.; Journal of Physics: Conference Series 786, 012020, 2017.