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المقاله
1 - An Efficient Green Synthesis of Copper Oxide NanoCrystallineInternational Journal of Bio-Inorganic Hybrid Nanomaterials , العدد 2 , السنة 4 , بهار 2015In this study, a feasible green method for the synthesis of copper oxide nanocrystalline is described by using sour cherry juice which has a significant effect on crystalline size, and morphology. The benefits of the green method, not only nanometer scale are formed but أکثرIn this study, a feasible green method for the synthesis of copper oxide nanocrystalline is described by using sour cherry juice which has a significant effect on crystalline size, and morphology. The benefits of the green method, not only nanometer scale are formed but also low-cost method are obtained in a normal atmosphere which it has been used (CH3COO)2Cu.H2O individually as Cu sources. All samples have calcination in 600°C. The effect of sour cherry juice concentration to control crystal growth is investigated by changing the amount of it to 20, 40, and 80 mL, respectively. The synthesized particles are characterized by using X-ray Diffraction (XRD) and Field Emission Scanning Electron Microscopy (FE-SEM). Powder X-ray Diffraction analysis confirms that pure Copper Oxide nanocrystallines are in a single phase monoclinic structure which the average crystalline size has estimated via Williamson-Hall plot from the highest peak of the XRD was among 15-55 nm for all samples. تفاصيل المقالة -
المقاله
2 - Magnetic and Structural Characteristics of Fe2O3 Nanostructure Synthesized in the Presence of Sour Cherry JuiceJournal of Advanced Materials and Processing , العدد 4 , السنة 4 , تابستان 2016T The nanostructures of Fe2O3 have been synthesized applying sour cherry juice and iron chloride as a low-cost and eco-friendly method at ambient conditions. Sour cherry juice has been used as a surfactant and the kind of surfactant had an important effect on the size أکثرT The nanostructures of Fe2O3 have been synthesized applying sour cherry juice and iron chloride as a low-cost and eco-friendly method at ambient conditions. Sour cherry juice has been used as a surfactant and the kind of surfactant had an important effect on the size and morphology of the products. The effect of sour cherry juice concentration and calcination temperature on the morphologies of Fe2O3 nanostructures has been investigated. The prepared nanoparticles were subjected to X-ray diffraction (XRD) analysis, field emission scanning electron microscopy (FE-SEM), and vibrating sample magnetometer (VSM) system. The powder X-ray diffraction analysis confirmed that Fe2O3 nanostructures are in Rhombohedral and Cubic phases. The average crystalline size estimated by the Williamson-hall method was about 13-32 nm for all samples. Various morphologies were also obtained by changing the amount of sour cherry juice. The saturation magnetization increased with the growth of crystals. تفاصيل المقالة -
المقاله
3 - A facile one-pot four-component synthesis of dihydropyrrol-2-ones using Cl3CCO2HIranian Journal of Catalysis , العدد 1 , السنة 5 , زمستان 2015A convenient synthesis of different types of polyfunctional dihydropyrrol-2-ones via one-pot four component reactions of formaldehyde, dialkyl acetylenedicarboxylates and amines, catalyzed by trichloroacetic acid (Cl3CCO2H) at room temperature has been investigated. The أکثرA convenient synthesis of different types of polyfunctional dihydropyrrol-2-ones via one-pot four component reactions of formaldehyde, dialkyl acetylenedicarboxylates and amines, catalyzed by trichloroacetic acid (Cl3CCO2H) at room temperature has been investigated. The significant advantages of this synthetic method are mild reaction conditions, available and inexpensive material, short reaction times, good yields, simple work-up. تفاصيل المقالة -
المقاله
4 - Maltose as a green catalyst for the synthesis of 3,4,5-substituted furan-2(5H) ones in waterFaranak Farhadpour Nourallah Hazeri Sajjad Salahi Parvaneh Dastoorani Razieh Doostmohammadi Mojtaba Lashkari Majid Ghashang Malek Taher MaghsoodlouIranian Journal of Catalysis , العدد 5 , السنة 4 , پاییز 2014Maltose as an efficient, available, cheap and eco-friendly catalyst has been applied for the synthesis of 3,4,5-substituted furan-2(5H)one derivatives via a one-pot three-component reaction of arylamines, aromatic aldehydes and dialkyl acetylenedicarboxylates in water. أکثرMaltose as an efficient, available, cheap and eco-friendly catalyst has been applied for the synthesis of 3,4,5-substituted furan-2(5H)one derivatives via a one-pot three-component reaction of arylamines, aromatic aldehydes and dialkyl acetylenedicarboxylates in water. This method has notable advantages in terms of simple workup, no need for column chromatography, short reaction time and high yields. تفاصيل المقالة -
المقاله
5 - Multi-component preparation of diethyl/methyl 1,3-diaryl-1,2,3,6-tetrahydro-pyrimidine-4,5-dicarboxylates using hydrated phosphomolybdic acid as an efficient catalystIranian Journal of Catalysis , العدد 2 , السنة 5 , بهار 2015The synthesis of diethyl/methyl 1,3-diaryl-1,2,3,6-tetrahydro-pyrimidine-4,5-dicarboxylates can be achieved using one-pot reaction from dialkylacetylene dicarboxylate, amines, and formaldehyde by employing hydrated phosphomolybdic acid (H3[P(Mo3O10)4].xH2O) as catalyst أکثرThe synthesis of diethyl/methyl 1,3-diaryl-1,2,3,6-tetrahydro-pyrimidine-4,5-dicarboxylates can be achieved using one-pot reaction from dialkylacetylene dicarboxylate, amines, and formaldehyde by employing hydrated phosphomolybdic acid (H3[P(Mo3O10)4].xH2O) as catalyst at room temperature. The effect of various solvent and catalyst amount was investigated. The salient features of the present method are: simple and straightforward work-up, cost-effective and environmentally benign procedure. The obtained yield of products was in the range of 75-92%. Based on the obtained results, the steric effects of the substituents in dialkylacetylene dicarboxylates played significant role in the rate of the reaction. When diethylacetylene dicarboxylate were used in this process, the corresponding product was obtained in good yields but in longer reaction time. Electron donating group on the amine was able to facilitate the transformation by giving evidently shorter reaction times. تفاصيل المقالة -
المقاله
6 - An efficient synthesis of 4-aryl-7-benzylidene-hexahydro-2H-cyclopenta[d] pyrimidin-2-ones/thiones catalyzed by p-dodecylbenzenesulfonic acidIranian Journal of Catalysis , العدد 2 , السنة 5 , بهار 2015A new and efficient method has been developed for the synthesis of 4-aryl-7-benzylidene-1,3,4,5,6,7-hexahydro-2H-cyclopenta[d]pyrimidin-2-ones through Biginelli-like reaction of cyclopentanone, with urea/thiourea and aromatic aldehyde employing p-dodecylbenzenesulfonic أکثرA new and efficient method has been developed for the synthesis of 4-aryl-7-benzylidene-1,3,4,5,6,7-hexahydro-2H-cyclopenta[d]pyrimidin-2-ones through Biginelli-like reaction of cyclopentanone, with urea/thiourea and aromatic aldehyde employing p-dodecylbenzenesulfonic acid (DBSA) as a recyclable catalyst under solvent-free condition. The recovered catalyst was recycled for further runs. The product formation takes place via a cross-aldol condensation of benzaldehyde with cyclopentanone in the presence of DBSA to produce benzylidene intermediate and subsequent Michael addition. The present approach offers the advantages of short reaction time, mild reaction conditions, high yields and convenient operation. All the products were obtained in good to excellent yields and the structures of the synthesized compounds were established by advanced spectroscopic data. تفاصيل المقالة -
المقاله
7 - Multi-component, one-pot, aqueous media preparation of dihydropyrano[3, 2-c]chromene derivatives over MgO nanoplates as an efficient catalystIranian Journal of Catalysis , العدد 4 , السنة 6 , تابستان 2016Red pine leafs were applied for the green method preparation of MgO nano-plates. The MgO nano-plates were used for the one-pot synthesis of dihydropyrano [3,2-c] chromene derivatives. This procedure is very simple and affords excellent yields. MgO nanoplates were synthe أکثرRed pine leafs were applied for the green method preparation of MgO nano-plates. The MgO nano-plates were used for the one-pot synthesis of dihydropyrano [3,2-c] chromene derivatives. This procedure is very simple and affords excellent yields. MgO nanoplates were synthesized via a simple precipitation method with the using of an extract solution of red pine leaves. The XRD pattern shows a cubic phase ofMgO . Field Emission Scanning Electronic Microscopy (FE-SEM) shows clearly that the surface of the as-prepared MgO nano-plates have a homogeneous microstructure made up of layers of various sizes and forms. The plates form irregular grains with a lateral size of 40-110 nm. تفاصيل المقالة -
المقاله
8 - Alkyl Ammonium Tungstate Bonded to Fe3O4@SiO2 Nanoparticles; a highly efficient Catalyst for the Oxidation of Symmetrical Sulfides to Symmetrical SulfoxidesIranian Journal of Catalysis , العدد 5 , السنة 13 , پاییز 2023A magnetic organic-inorganic hybrid of Fe3O4@SiO2-functionalized propylpiperazine-1,4-diium tungstate (A) nanoparticles with a spherical structure was prepared and completely characterized by XRD, SEM, TGA-DTA, and FT-IR spectral techniques. The magnetic hybrid was used أکثرA magnetic organic-inorganic hybrid of Fe3O4@SiO2-functionalized propylpiperazine-1,4-diium tungstate (A) nanoparticles with a spherical structure was prepared and completely characterized by XRD, SEM, TGA-DTA, and FT-IR spectral techniques. The magnetic hybrid was used in the oxidation of symmetrical sulfides to symmetrical sulfoxides under ambient conditions. The excellent yields of sulfoxides, easy operation, and recovery, magnetic properties of the catalyst, and environmentally friendly system are the key advantages of this method. تفاصيل المقالة -
المقاله
9 - Preparation of 1,5-diaryl-3-(arylamino)-1H-pyrrol- 2(5H)-one derivatives using 1-methylpiperidinium hydrogen sulfate as an efficient catalystJournal of the Iranian Chemical Research , العدد 2 , السنة 5 , بهار 2012A highly efficient and environmentally friendly synthesis of various 1,5-diaryl-3-(arylamino)-1H-pyrrol-2(5H)-ones catalyzed by 1-methylpiperidinium hydrogen sulfate via one-pot cyclo-condensation reaction ofaldehydes, amines and ethyl 2-oxopropanoate under ambient cond أکثرA highly efficient and environmentally friendly synthesis of various 1,5-diaryl-3-(arylamino)-1H-pyrrol-2(5H)-ones catalyzed by 1-methylpiperidinium hydrogen sulfate via one-pot cyclo-condensation reaction ofaldehydes, amines and ethyl 2-oxopropanoate under ambient conditions has been explored. The presentmethodology offers several advantages such as good yields, simple procedure, shorter reaction times andmilder conditions and the products were purified without resorting to chromatography. تفاصيل المقالة
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