Highly Porous Bi(III) Modified Rice Husk Silica Photocatalyst for the Photocatalytic Removal of Cationic Methylene Blue

الموضوعات : Iranian Journal of Catalysis

Normawati Jasni ¹ , Anwar Iqbal ² , N. H. H Abu Bakar ³ , Dede Heri Yuli Yanto ⁴ , Hor Jia Yi ⁵ , Noor Haida Mohd Kaus ⁶ , Mohd Norazmi Ahmad ⁷ , Sri Mulijani ⁸

1 - School of Chemical Sciences, Universiti Sains Malaysia, 11800 USM, Penang, Malaysia
2 - School of Chemical Sciences, Universiti Sains Malaysia, 11800 USM, Penang, Malaysia
3 - School of Chemical Sciences, Universiti Sains Malaysia, 11800 USM, Penang, Malaysia
4 - Research Center for Applied Microbiology, National Research and Innovation Agency (BRIN), Cibinong, Bogor 16911, Indonesia
5 - School of Chemical Sciences, Universiti Sains Malaysia, 11800 USM, Penang, Malaysia
6 - School of Chemical Sciences, Universiti Sains Malaysia, 11800 USM, Penang, Malaysia
7 - Experimental and Theoretical Research Lab, Department of Chemistry, Kulliyyah of Science, International Islamic University Malaysia, Bandar Indera Mahkota, 25200 Kuantan, Pahang, Malaysia
8 - Department of Chemistry, Bogor Agriculture University-Bogor-Indonesia, Indonesia

تاريخ الإرسال : 13 الإثنين , محرم, 1445 تاريخ التأكيد : 08 السبت , ربيع الأول, 1445 تاريخ الإصدار : 16 الجمعة , صفر, 1445

الکلمات المفتاحية: Methylene Blue, Photocatalyst, Bismuth, Mesoporous silica, Rice husk, Sunlight,

ملخص المقالة :

A series of bismuth-silicate photocatalysts were synthesized via the sol-gel method for photodegradation of methylene blue (MB) under sunlight irradiation, utilizing rice husk ash as a silica precursor. The scanning electron microscopy/energy dispersive X-ray (SEM/EDX) analysis detected Bi content in 3-10 wt% range. Furthermore, it can be seen that the porosity decreased as the Bi concentration increased. The N2 adsorption-desorption analysis indicates the presence of mesopores with an average diameter of 297-554 Å with Brunauer–Emmett–Teller (BET) surface area of 5.6-30.5 m2/g. The photocatalyst with a Bi concentration of 4 wt% (RHSBi-A2) was the most active in the photodegradation of MB; the removal reached 90% within 4 h. The photodegradation is proposed to be driven by superoxide ( ), hydroxyl (•OH) radicals, and hole (h+) based on the valence band (VB) and conduction band (CB) potentials. The porous silica framework is proposed to act as an electron reservoir, allowing better MB adsorption and enhancing light absorption.

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