Fracture surface

دسترسی آزاد مقاله

1 - Preparation of Nitrogen-Doped Graphene Aerogel/Epoxy Nanocomposites and Experimental Study of Mechanical Properties
ali kordi saeed adibnazari Ali Imam mohammad najafi maryam ghasabzadeh saryazdi

10.30495/admt.2020.1904850.1205

Nitrogen-Doped Graphene Aerogel (N-GA) nanomaterials can significantly improve the functional efficiency of polymer composites due to its three-dimensional structure and suitable physical properties. The preparation process affects the performance improvement. In this s چکیده کامل

Nitrogen-Doped Graphene Aerogel (N-GA) nanomaterials can significantly improve the functional efficiency of polymer composites due to its three-dimensional structure and suitable physical properties. The preparation process affects the performance improvement. In this study, the effect of preparation method and the mechanisms affecting the strength behavior of Nitrogen-doped Graphene Aerogel/Epoxy (N-GA/E) nanocomposites was investigated. For this purpose, nanoparticles of Graphene Oxide (GO) were produced using Hummers’ method; then, the N-GA was synthesized using the hydrothermal method and the freeze-drying process. The characterization experiments were used in order to confirm the structure and quality of the synthesized nanomaterials. Then, specimens of nanocomposite were prepared by adding weight percentages of 0.05, 0.1, 0.2, 0.5, 1, and 2 from the synthesized N-GA to the epoxy resin. In other preparation processes, N-GA/E nanocomposite specimens were produced using auxiliary solvents. After tensile tests, the best strength performance was observed in the specimens with the preparation process in which acetone solvent was used. The tensile strength and modulus of these nanocomposite specimens have increased by 23% and 20% compared to neat epoxy specimens, respectively. Also, the optimal weight percentage of N-GA nanomaterials for distribution in epoxy is 0.1 wt.%. Microscopic images of the fracture surfaces of the specimens used in the tensile test showed that the placement of N-GA porous plates in epoxy with the creation of the mechanism for micro crack formation led to more energy absorption during the stretching process of the N-GA/E nanocomposites. پرونده مقاله

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2 - Investigation of mechanical properties and fracture surfaces of 5086 Al-based alloy processed by equal channel angular pressing in different routes
Seyed Elias Mousavi Mohammad Hossein Khaleghifar Farshid Ahmadi Mahmood Meratian

Equal channel angular pressing has been among prominent part of procedures employed for the fabrication of the ultraﬁne-grained structures of various severe plastic deformation techniques. The objective of this paper was to experimentally investigate the inﬂuence of the چکیده کامل

Equal channel angular pressing has been among prominent part of procedures employed for the fabrication of the ultraﬁne-grained structures of various severe plastic deformation techniques. The objective of this paper was to experimentally investigate the inﬂuence of the process in the two rotational routes A and Bc on the mechanical properties of Al 5086 alloy. Specimens were processed up to 10 passes at 150 ºC in a die with 120º internal angle. To evaluate the mechanical properties, uni-axial tensile and hardness tests were performed on the specimens. The results showed that in all passes, the route Bc had a higher effect on the simultaneous improvement of strength, elongation, and hardness. Investigation of the fracture surface using Scanning Electron Microscopy revealed that increasing the number of passes led to raising the number of dimples and the better distribution of them for both routes. The textures were also studied using the X-ray diffraction patterns. The results showed the dominant texture was altered from (111) to (220) plane by increasing the number of passes through both routs. پرونده مقاله

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3 - Fatigue and corrosion fatigue properties of Ti-6Al-4V implant grade titanium alloy in Ringer solution
Mahmoud Hajisafari Arman Zare Bidaki Saeid Yazdani

Nowadays modification of metallic biomaterials which are used as implants for bone and hard tissues replacement is considered as an important subject. In the current study, corrosion fatigue properties of Ti-6Al-4V alloy investigated via Rotating-Bending standard test m چکیده کامل

Nowadays modification of metallic biomaterials which are used as implants for bone and hard tissues replacement is considered as an important subject. In the current study, corrosion fatigue properties of Ti-6Al-4V alloy investigated via Rotating-Bending standard test method and then, the results compared with the fatigue properties of the specimens tested in the same conditions. Scanning electron microscopy used to investigate the chemical composition (EDS- Energy-dispersive X-ray spectroscopy), microstructural features and crack propagation characteristics. Results showed that the presence of corrosive environment not only results in decrease in fatigue life, but also eliminates the fatigue limit. Further studies revealed that aggregation of corrosion products, with more hardness values, at the crack tip cause an obvious deviation of crack propagation from its main direction. Therefore, a tortuous crack path through the bulk of the specimens was detected concurrent with penetration of solution into the crack. In addition, dimensions and morphology of fatigue crack surfaces were completely different from corrosion fatigue cracks as well. پرونده مقاله

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4 - Investigating the Effects of Boron and Zirconium on the High-Temperature Fatigue Behavior of Nimonic 105 Super Alloy
Zahra Asghary Masumeh Seifollahi Maryam Morakabati Seyed Mahdi Abbasi

This study investigates the low-cycle fatigue of Nimonic105 alloy with boron and zirconium of 0.003-0.013 wt.% and 0.0-0.16 wt.%, respectively at 750 °C. The fatigue test results indicated that the alloy with boron of 0.013 wt.% had the highest fatigue life of 400 c چکیده کامل

This study investigates the low-cycle fatigue of Nimonic105 alloy with boron and zirconium of 0.003-0.013 wt.% and 0.0-0.16 wt.%, respectively at 750 °C. The fatigue test results indicated that the alloy with boron of 0.013 wt.% had the highest fatigue life of 400 cycles, while the base alloy showed the lowest fatigue life of 21 cycles at 2% strain amplitudes. For the alloy with 0.16 wt.% Zr, and the alloy with 0.08 wt.% Zr and 0.006 wt.% B, cyclic-hardening occurred at a constant slope. Then, hardening followed a nonlinear procedure at a reducing rate. Finally, softening and fracture happened. For 0.013 wt.% Zr alloy, however, the diagram reached a stable state or slow cyclic-softening and failed after a relatively short period of cyclic -softening. The Coffin-Manson equations’ parameters verified the increased flexibility due to the addition of B. to be a factor in improving high-temperature LCF strength. The investigation of the samples’ fracture surfaces indicated that the intergranular fracture of the base alloy with the lowest fatigue life became intergranular and transgranular fracture in the alloy with 0.16 ‌wt.% Zr content and the alloy with 0.08 wt.% Zr content and 0.006 wt.% B contents. Also, 0.013 wt.% B alloy with the highest fatigue life showed a completely transgranular fracture. پرونده مقاله

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5 - مورفولوژی سطح شکست و ارتباط آن با چقرمگی/انعطاف پذیری در شیشه فلز حجمی آلیاژ Zr46(Cu4.5/5.5Ag1/5.5)46Al8
محمدتقی اسدی خانوکی

هدف از این پژوهش بررسی رفتار شکست و پدیده‌ی تبدیل نرمی به تردی در یک شیشه‌فلز حجمی آلیاژ پایه‌ی زیرکونیم است. همچنین به-طور خاص ارتباط بین مورفولوژی‌های سطح شکست و چقرمگی و انعطاف‌پذیری بررسی شده است. به همین منظور با استفاده از فرآیند ذوب قوسی و ریخته‌گری مکشی در خلأ، چکیده کامل

هدف از این پژوهش بررسی رفتار شکست و پدیده‌ی تبدیل نرمی به تردی در یک شیشه‌فلز حجمی آلیاژ پایه‌ی زیرکونیم است. همچنین به-طور خاص ارتباط بین مورفولوژی‌های سطح شکست و چقرمگی و انعطاف‌پذیری بررسی شده است. به همین منظور با استفاده از فرآیند ذوب قوسی و ریخته‌گری مکشی در خلأ، آلیاژ آمورف تولید و در نرخ mm/min 2/0 و دماهای 77 و 298 کلوین تحت آزمون خمش سه-نقطه‌ای قرار گرفت. سطوح شکست به کمک SEM مورد مطالعه و ارزیابی قرار گرفتند و با استفاده از مدل ناپایداری انحنای جریان، ضمن تعیین چقرمگی آلیاژ مورد مطالعه از طریق محاسبه‌ی اندازه‌ی مورفولوژی سطح شکست، ساز و کار شکست ترد و نرم بررسی شد. در ادامه، شرایط و دلایل تشکیل مورفولوژی‌های مختلف در این دو حالت به‌صورت کمّی تعیین گردید. نتایج نشان می‌دهد که آلیاژ پایه‌ی زیرکونیم علی‌رغم نرم بودن در دمای اتاق، در دماهای بسیار پایین (77 کلوین) به‌شدت ترد و بیان‌گر رفتار تبدیل نرمی به تردی است. تحت این شرایط میزان متوسط چقرمگی شکست از حدود MPa.m1/2 16 در دمای اتاق به حدود MPa.m1/2 5/3 در دمای 77 کلوین کاهش یافت. همچنین با کمک مدل ناپایداری انحنای جریان و اطلاعات سطح شکست، طول موج اعوجاج بحرانی (λc) برای این آلیاژ nm 127 محاسبه شد. درصورتی که طول موج اعوجاج اولیه (λI) کمتر از این مقدار بحرانی باشد، مشخصه‌ی سطح شکست به صورت نانو شیارهای موازی و متناوب خواهد بود. در صورتی که λI بزرگتر از مقدار بحرانی باشد شرایط برای تشکیل طرح دیمپل و طرح رگه‌ای فراهم خواهد شد. پرونده مقاله

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