Synthesis of Single-Crystalline Octahedral Co3O4 with Solid-State Thermal Decomposition

محورهای موضوعی : پلیمر

Aliakbar Dehno Khalaji ¹ ()

تاریخ دریافت : 1394/08/20 تاریخ پذیرش : 1394/08/20 تاریخ انتشار : 1393/10/11

کلید واژه:

چکیده مقاله :

In this paper, single crystalline octahedral Co3O4with dimensions about 100–500 nm and smooth surface has been prepared by solid-state thermal decomposition of cobalt(II) Schiff base complex Co((3,4-MeO-ba)2en)Cl2as new precursor at 450ºC under air atmosphere for 3.5 h. Surface morphology of the products were characterized by Fourier transform infrared spectroscopy (FT-IR), X-ray powder diffraction (XRD) and scanning electron microscopy (SEM).