The comparison synthesis of CuNiO2 nanoparticles prepared by sol-gel auto-combu on, microwave and co-precipitation techniques
محورهای موضوعی : Journal of Physical & Theoretical Chemistry
S. A. Khorrami
1
(-)
N. Naderfa
2
(-)
M. G. G Mojadad
3
(-)
کلید واژه: Sol-gel auto-combustion, Co-precipitation: Microwave, SEM, XRD,
چکیده مقاله :
The CuNiCA nanopanicles have been synthesized by sol-gel auto-combusson. microwave and co-precipitationtechniques. Then, the results of the three techniques were compared. In the vol-ael auto-combustion synthesiswas used glycine as a fuel. At first, sol was prepared. Then, gel was achieved from drying so'. The prepared gelwas burnt at 350°C. In the noicrowavc technique, gel was prepared. Then, the final nanoparticles were producedon influence of microwave irradiation. The CuNiO2 nanoparticles 'ere prepared by co-pAcipitation methodinvolved metal sulfates The temperature of calcmations was 620T. These minoparticles were investigated byX-ray diffraction (XRD) and Scanning Plectmn Microscopy (SEM) techniques. The XRD results show that thenangeryssil eon tat iis various phases. stnictures and the average size of MilliThIMCIIMA CuNi0: cry stallities wascalculated by Scherer equation. Scanning Electron Microscopy was also used to characterize the microstnic tareand morphology.
