The Evaluation of MAR-M247 Microstructural Changes after Standard Heat Treatment and Creep Test
محورهای موضوعی : Journal of Environmental Friendly Materialsآرمان ربیعی فر 1 , Mostafa Erfan 2 , Narges Shahidi 3
1 - مرکز تحقیقات مواد مهندسی پیشرفته دانشگاه آزاد اسلامی واحد کرج
2 - Advanced Materials Engineering Research Center, Karaj Branch, Islamic Azad University, Karaj, Iran
3 - Advanced Materials Engineering Research Center, Karaj Branch, Islamic Azad University, Karaj, Iran
کلید واژه: MAR-M247 Superalloy, Creep, Microstructure, Heat Treatment,
چکیده مقاله :
The cast nickel-base MAR-M247 superalloy has been widely used for high-temperature components. In this work, the creep and room temperature tensile behavior of MAR-M247 superalloy after dual-stage standard heat treatment is evaluated. The microstructure of heat-treated superalloy consists of a matrix with a -eutectic, strengthening cubic precipitates, and particulate, script-like carbides at the grain boundaries (GBs). Under the creep testing conditions in this study, the volume fraction and primary gamma prime size increased; the script-like MC carbide along the GB elongated, and the TCP phase formed in the vicinity of grain boundary carbides. On the other hand, during the creep test, the thin film formed around the gamma prime phase became thicker, causing an increase in the toughness of the superalloy and an expansion of the steady-state stage in the creep curve.
The cast nickel-base MAR-M247 superalloy has been widely used for high-temperature components. In this work, the creep and room temperature tensile behavior of MAR-M247 superalloy after dual-stage standard heat treatment is evaluated. The microstructure of heat-treated superalloy consists of a matrix with a -eutectic, strengthening cubic precipitates, and particulate, script-like carbides at the grain boundaries (GBs). Under the creep testing conditions in this study, the volume fraction and primary gamma prime size increased; the script-like MC carbide along the GB elongated, and the TCP phase formed in the vicinity of grain boundary carbides. On the other hand, during the creep test, the thin film formed around the gamma prime phase became thicker, causing an increase in the toughness of the superalloy and an expansion of the steady-state stage in the creep curve.
[1] Bor HY, Wei CN, Jeng RR, Ko PY, Elucidating the Effects of Solution and Double Ageing Treatment on the Mechanical Properties and Toughness of MAR-M247 Superalloy at High Temperature. Mater. Chem. Phys.2008; 109(2-3):334–341.
[2] Nathal MV, Maier RD, Ebert LJ, The influence of cobalt on the tensile and stress-rupture properties of the nickel-base superalloy mar-m247. Metall. Trans. A 1982; 13:1767–1774.
[3] Nathal MV, Maier RD, Ebert LJ, The Influence of Cobalt on the Microstructure of the Nickel-Base Superalloy MAR-M247. Metall. Trans. A 1982; 13:1775–1783.
[4] Bor HY, Chao CG, Ma CY, The effects of Mg microaddition on the mechanical behavior and fracture mechanism of MAR-M247 superalloy at elevated temperatures. Metall. Trans. A 1999; 30:551–561.
[5] Bor HY, Chao CG, Ma CY, The influence of Mg on creep properties and fracture behaviors of Mar-M247 superalloy under 1255 K/200 MPa. Metall. Trans. A 2000; 31:1365–1373.
[6] Kattus JR, MAR M 247—Aerospace Structural Metals Handbook. West Lafayette: Purdue Research Foundation; 1999.
[7] Szczotok A, Szala J, Cwajna J, Hetmanczyk M, Selection of Etching Methods of Primary Carbides in MAR-M247 Nickel-Base Superalloy for Computer-Aided Quantitative Metallography. Mater. Charact. 2006; 56(4-5):348–354.
[8] Bor HY, Chao CG, Ma CY, The Influence of Magnesium on Carbide Characteristics and Creep Behavior of the MAR-M247 Superalloy. Scr. Mater. 1998; 38(2):329–335.
[9] Murakurrno T, Kobayashi T, Koizumi Y, Harada H, Creep Behavior of Ni-base Single Crystal Superalloy with Various Volume Fraction. Acta Mater. 2004; 52(12):3737–3744.
[10] Allied-Signal Aerospace Company: Engine Materials Specification 55447, Castings, Investment, MAR-M247, 1988.
[11] Bhaumik SK, BhaskaranTA, Rangaraju R, Wenkataswamy MA, Parameswara MA, Krishnan RV, Failure of Turbine Rotor Blisk of an Aircraft Engine. Eng. Fail. Anal. 2002; 9(3):287–301.
[12] Zeisler-Mashl KL, Pletka BJ, Segregation During Solidification in the MAR-M247 system, International Symposium on Superalloys, Warrendale, PA, 1992; 175–184.
[13] Ruusing J, Wanderka N, Czubayko U, Naundorf V, Mukherji D, Rosler J, Rhenium distribution in the matrix and near the particle–matrix interface in a model Ni–Al–Ta–Re superalloy. Scr. Meter. 2002; 46(3):235–240.
[14] Wei CN, Bor HY, Chang L, Effect of Hot Isostatic Pressing on Microstructure and Mechanical Properties of CM-681LC Nickel-Base Superalloy Using Microcast. Mater. Trans. 2008; 49:193–201.
[15] Huang HE, Koo CH, Effect of Zirconium on Microstructure and Mechanical Properties of Cast Fine-Grain CM 247 LC Superalloy. Mater. Trans. 2004; 45(2):554–561.
[16] Liu LR, Jin T, Zhao NR, Sun XF, Guan HR, Hu ZQ, Formation of carbides and their effects on stress rupture of a Ni-base single crystal superalloy. Mater. Sci. Eng. A 2003; 361(1-2):191–197.
[17] Liu LR, Jin T, Zhao NR, Wang ZH, Sun XF, Guan HR, ZQ Hu, Effect of carbon addition on the creep properties in a Ni-based single crystal superalloy. Mater. Sci. Eng. A 2004; 385(1-2):105–112.
[18] Kotval PS, Venables JD, Calder RW, The role of hafnium in modifying the microstructure of cast nickel-base superalloys. Metall. Trans. 1972; 3:453–458.
[19] Gell M, Kortovich CS, Bricknell RH, Kent WB, Radavich JF (Eds.), Proceedings of Superalloys, AIME, Warrendale, PA, 1984; 43–52.
[20] Floreen S, Superalloys Mechanical behaviour, John Wiley & Sons, New York, 1987; 241–262.
[21] Coakley J, Lass EA, Ma D, Frost M, Stone HJ, Seidman DN, Dunand DC, Lattice parameter misfit evolution during creep of a cobalt-based superalloy single crystal with cuboidal and rafted gamma-prime
microstructures. Acta Mater. 2017; 136:118-125.
[22] Chen J, Lee JH, Jo CY, Choe SJ, Lee YT, MC carbide formation in directionally solidified MAR-M247 LC superalloy. Mater. Sci. Eng. A, 1998; 247(1-2):113–125.
[23] Tsai YL, Wang SF, Bor HY, Hsu YF, Effects of alloy elements on microstructure and creep properties of fine-grained nickel-based superalloys at moderate temperatures. Mat. Sci.Eng. A 2013; 571:155–160.
[24] Sims CT, Stoloff NS, Hagel WC, Superalloys II, John Wiley & Sons, New York, 1987; 255–256.
[25] Baldan R, Rocha RLP, Tomasiello RB, Nunes CA, Silva Costa AM, Barboza MJR, Coelho GC, Rosenthal R, Solutioning and Aging of MAR-M247 Nickel-Based Superalloy, J. Mater. Eng. Perform. 2013;22:2574–2579.
[26] Bor HY, Wei CN, Jeng RR, Ko PY, Elucidating the effects of solution and double aging treatment on the mechanical properties and toughness of MAR-M247 superalloy at high temperature. Mater. Chem. Phys. 2008; 109(2-3):334–341.
[27] Koul AK, Wallace W, A note on the microstructural dependence of creep strength in Inconel 700. Met. Trans. A 1982; 13:673–675.
[28]Liao JH, Bor HY, Wei CN, Chao CG, Liu TF, Influence of microstructure and its evolution on the mechanical behavior of modified MAR-M247 fine-grain superalloys at 871 °C. Mater. Sci.
Eng. A 2012; 539:93–100.