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  • Diisopropyl Ether Production via Isopropanol Catalytic Dehydration over Zirconium Phosphate Modified Natural Zeolite

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کد مقاله : IJC-2208-1961 (R1) بازدید : 150 صفحه: 463 - 474

10.30495/ijc.2022.1965421.1961

نوع مقاله: پژوهشی

Diisopropyl Ether Production via Isopropanol Catalytic Dehydration over Zirconium Phosphate Modified Natural Zeolite

محورهای موضوعی : Iranian Journal of Catalysis

Hasanudin Hasanudin 1 , Wan Asri 2 , Jeniva Anindia 3 , Suheryanto Suheryanto 4 , Zainal Fanani 5 , Nino Rinaldi 6 , Muhammad Al Muttaqii 7

1 - Department of Chemistry, Faculty of Mathematics and Natural Science, Universitas Sriwijaya, Indralaya 30662, Indonesia|Biofuel Research Group, Faculty of Mathematics and Natural Science, Universitas Sriwijaya, Indralaya 30662, Indonesia
2 - Department of Chemistry, Faculty of Mathematics and Natural Science, Universitas Sriwijaya, Indralaya 30662, Indonesia|Biofuel Research Group, Faculty of Mathematics and Natural Science, Universitas Sriwijaya, Indralaya 30662, Indonesia
3 - Department of Chemistry, Faculty of Mathematics and Natural Science, Universitas Sriwijaya, Indralaya 30662, Indonesia|Biofuel Research Group, Faculty of Mathematics and Natural Science, Universitas Sriwijaya, Indralaya 30662, Indonesia
4 - Department of Chemistry, Faculty of Mathematics and Natural Science, Universitas Sriwijaya, Indralaya 30662, Indonesia|Biofuel Research Group, Faculty of Mathematics and Natural Science, Universitas Sriwijaya, Indralaya 30662, Indonesia
5 - Department of Chemistry, Faculty of Mathematics and Natural Science, Universitas Sriwijaya, Indralaya 30662, Indonesia|Biofuel Research Group, Faculty of Mathematics and Natural Science, Universitas Sriwijaya, Indralaya 30662, Indonesia
6 - Research Center for Chemistry, National Research and Innovation Agency(BRIN-Indonesia), Science and Technology Park B.J. Habibie, Serpong, South Tangerang 15314, Banten Indonesia
7 - Research Center for Chemistry, National Research and Innovation Agency(BRIN-Indonesia), Science and Technology Park B.J. Habibie, Serpong, South Tangerang 15314, Banten Indonesia

تاریخ دریافت : 1401/05/22 تاریخ پذیرش : 1401/09/21 تاریخ انتشار : 1401/10/10

کلید واژه: zeolite, Modification, zirconium phosphate, isopropanol conversion, diisopropyl ether,

چکیده مقاله :

In this work, diisopropyl ether (DIPE) was produced through catalytic dehydration of isopropanol over zirconium phosphate-modified phosphate modified natural zeolite. The catalyst was prepared via the wet impregnation method. They were tested at 150 ˚C for 3 hours under a reflux system. The effect of zeolite-Zr(H2PO4)4 metal loading and zeolite-Zr without phosphate incorporation on dehydration isopropanol was also assessed. The results showed the natural zeolite was successfully modified as confirmed by XRD, FTIR, SEM-EDX, N2 physisorption, and catalyst acidity by the gravimetric technique. The highest isopropanol conversion (66.73%) was accomplished by 8 mEq/g zeolite-Zr(H2PO4)4 followed by the DIPE yield and selectivity up to 35.81% and 47.8%, respectively. Further reusability investigation showed that zeolite-Zr(H2PO4)4 catalyst provided adequate reusability up to the fourth reused with relatively decreased catalytic activity towards isopropanol dehydration.

چکیده انگلیسی:

منابع و مأخذ:


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