Synthesis, characterization, and antibacterial activities investigation of zinc (II) oxide nanorods, bulk and nanoscale of coordination polymer as precursor

Subject Areas :

آرزو کمالی ¹ , الهام رضوان نژاد ² , زهره رشیدی رنجبر ^{3 *}

1 - کارشناس ارشد نانوشیمی، دانشکده علوم، دانشگاه شهید باهنر کرمان، کرمان، ایران
2 - استادیار بیوتکنولوژی دامی، دانشگاه تحصیلات تکمیلی ماهان، کرمان، ایران
3 - استادیار شیمی معدنی، بخش شیمی، دانشکده علوم، دانشگاه شهید باهنر کرمان، کرمان، ایران

Received: 2016-10-12 Accepted : 2017-11-12 Published : 2018-05-22

Keywords: sensor, Tin Dioxide, Additive materials,

Abstract :

In this work, a coordination polymer in bulk and nano-scale: ]Zn(3-bpdh)Cl2]n(1), with 3-bpdh=2,5-bis(3-pyridyl)-3,4-diaza-2,4 hexadiene ligand, has been synthesized and characterized by IR and NMR spectroscopies. The nanostructures of coordination polymer (1) were prepared by using ultrasonic waves and sonochemistry method, and the size and morphology of the particles were characterized by Scanning Electron Microscopy (SEM). The nanostructures were used as precursors to prepare zinc (II) oxide nanorods by thermolysis. The ZnO nanorods were identified and their diameters were estimated by XRD and SEM, respectively. Also, the ligand, bulk and nanoscales of coordination polymer (1) and zinc (ІІ) oxide nanorods have been screened for antibacterial activities against Bacillus alvei bacteria caused by honey bee European foulbrood disease. The Minimum Inhibitory Concentrations (MIC) has shown moderate antibacterial activities in comparison to some standard drugs

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