Evaluation of Flow Behavior of Novel Titanium Ti-3873 Alloy Via Compressive Deformation in Two Phase α/β and Single Phase β Regions
الموضوعات :Mahnaz Dabbaghi 1 , Maryam Morakabati 2
1 - Faculty of Materials and Manufacturing Thechnologies, Malek Ashtar University of Technology, Tehran, Iran
2 - Faculty of Materials and Manufacturing Technologies, Malek Ashtar University of Technology
الکلمات المفتاحية: Ti-3Al-8Mo-7V-3Cr alloy, recovery, recrystallization, activation energy, processing map,
ملخص المقالة :
Semi-stable β-titanium (Ti-3873) Ti-3Al-8Mo-7V-3Cr alloy with excellent workability properties has been designed based on high demanded aircraft Ti-5Al-5Mo-5V-3Cr alloy according to semi-experimental d-electron approach. The aim of the present research is to investigate the deformation behavior of Ti-3873 alloy via warm compression test. For this purpose, compression test has been conducted in the temperature range of 650-850 °C and strain rates of 0.001,0.1 and 1, 1 s-1 at dual phase α/β and single phase β regions. The test was continued up to plastic strain of 0.7. For establishing the relationship between the microstructure and flow behavior, the initial and subsequent microstructure of the specimens after warm deformation was studied via optical and scanning electron microscopes. The microstructural evaluation and flow curves revealed that dynamic recovery and partial continuous dynamic recrystallization were the dominant restoration mechanisms. The results showed that softening has been increased in the temperature range of 800-850 °C and strain of 0.001 and 0.1 s-1 which is confirmed by the activation energy calculated from the sinus hyperbolic equation. The activation energy for dual phase α/β and single phase β regions are determines as 429 kJ/mol and 353 kJ/mol, respectively. The higher value of activation energy for α/β dual phase region is attributed to dynamic globularization of α lamellas. The preferable regions for hot workability of the alloy were achieved at the temperature range of 800-850 °C and strain rate of 0.01-0.001 s-1 corresponding to the peak efficiency of 39% in the processing map.
[1] M. Abdel-Hady, K. Hinoshita and M. Morinaga "General approach to phase stability and elastic properties of β-type Ti-alloys using electronic parameters", Scr. Mater., Vol. 55, 2006, pp. 477–480.
[2] P. Lacombe, The 6th World Conference on Titanium. Cannes Paris. Les Edition de Physics. Part 4, 1989
[3] D. Kuroda, M. Niinomi, M. Morinaga, Y. Kato and T. Yashiro "Design and mechanical properties of new β type titanium alloys for implant materials", Mat. Sci. Eng. A, Vol. 243, 1998, pp. 244–24.
[4] S. Sadeghpour, S. M. Abbasi, M. Morakabati, L. P. Karjalainen and D. A. Porter "Effect of cold rolling and subsequent annealing on grain refinement of a beta titanium alloy showing stress-induced martensitic transformation" Mat. Sci. Eng. A, Vol. 731, 2018, pp. 465–478.
[5] S. Sadeghpour, S. M. Abbasi, M. Morakabati, A. L. P. Kisko, Karjalainen and D. A. Porter, "On the compressive deformation behavior of new beta titanium alloys designed by d-electron method", J. All. Comp., Vol. 746, 2018, pp. 206–217.
[6] F. S. Froes, "Titanium for medical and dental applications-An introduction. In Titanium in medical and dental applications. Australia. Elsevier. 2018
[7] S. Sadeghpour, S. M. Abbasi and M. Morakabati "Deformation-induced martensitic transformation in a new metastable β titanium alloy" J. All. Comp., Vol. 650, 2015, pp. 22–29.
[8] P. Laheurte, F. Prima, A. Eberhardt, T. Gloriant, M. Wary and E. Patoor "Mechanical properties of low modulus β titanium alloys designed from the electronic approach", J. Mech. Beh. Bio. Mat. 3, 2010, pp. 565–573.
[9] F. Sun, J. Y. Zhang, M. Marteleur, C. Brozek, E. F. Rauch, M. Veron and F. Prima, A new titanium alloy with a combination of high strength, high strain hardening and improved ductility, Scr. Mater., Vol. 94, 2015, 17-2.
[10] F. Chen, G. Xu, X. Zhang and K. Zhou, "Exploring the phase transformation in β-quenched Ti-5553 alloy during continuous heating via dilatometric measurement, microstructure characterization, and diffusion analysis", Metall. Mat. Trans. A, 2016, Vol. 47, pp. 5383–539.
[11] Y. Q. Jiang, Y. C. Lin, X. Y. Zhang, C. Chen, Q. W. Wang and G. D. Pang "Isothermal tensile deformation behaviors and fracture mechanism of Ti-5Al-5Mo-5V-1Cr-1Fe alloy in β phase field", Vacu., Vol 156, 2018, pp. 187-197.
[12] V. N. Moiseev,"Beta-titanium alloys and prospects of their development", Metal. Sci. Heat Treat., Vol. 40, 1998, pp. 482-485.
[13] G. Lütjering and J. C. Williams, "Titanium", 2007, Germany, Springer, p. 125.
[14] S. Sadeghpour, S. M. Abbasi, M. Morakabati and L. Karjalainen, "Effect of dislocation channeling and kink band formation on enhanced tensile properties of a new beta Ti alloy", J. Alloy. Comp., Vol. 808, 2019, 151741.
[15] S. M. Abbasi, M. Morakabati, A. H. Sheikhali and A. Momeni," Hot deformation behavior of beta titanium Ti-13V-11Cr-3Al alloy", Metall. Mate. Trans. A, Vol. 45, 2014, pp. 5201–5211.
[16] Y. C. Lin, J. Huang, H. B. Li and D. D. Chen, "Phase transformation and constitutive models of a hot compressed TC18 titanium alloy in the α+ β regime", Vacuu., Vol 157, 2018, pp. 83-91.
[17] S. M. Abbasi, A. Momeni, Y. C. Lin and H. R. Jafarian, "Dynamic softening mechanism in Ti-13V-11Cr-3Al beta Ti alloy during hot compressive deformation", Mat. Sci. Eng. A, Vol. 665, 2016, 154–160.
[18] A. Momeni, S. M. Abbasi and S. Sadeghpour, "Comparative study on the hot deformation behavior of Ti-5Al-5Mo-5V-3Cr and newly developed Ti-4Al-7Mo-3V-3Cr alloys", J. Vacuu. Vol. 161, 2019, pp. 410-418.
[19] X. Ma, W. Zeng, B. Xu, Y. Sun, C. Xue and Y. Han, "Characterization of the hot deformation behavior of a Ti–22Al–25Nb alloy using processing maps based on the Murty criterion", Interme, Vol. 20(1). 2012, pp. 1-7.
[20] Y. Zhu, W. Zeng, F. Feng and Y. Sun "Characterization of hot deformation behavior of as-cast TC21 titanium alloy using processing map" Mat. Sci. Eng. A, Vol. 528(3), 2011, pp. 1757-1763.
[21] G. E. Dieter, H. A. Kuhn and S. L. Semiatin, "Handbook of workability and process design", 2003ASM international, p. 214.
[22] M. Morakabati, H. Saki, R. Mahdavih, "effect of single-step and two-step aging on the microstructure and mechanical properties of the novel Ti-3Al-8Mo-7V-3Cr alloy", Modares Mech. Eng., 3, Vol. 23, 2023, pp. 199-208.
[23] R. L. Goetz and S. L. Semiatin, "The adiabatic correction factor for deformation heating during the uniaxial compression test" J. Mat. Eng. Perf., Vo. 10, 2001, pp. 710-717.
[24] Y. Han, W. Zeng, Y. Qi and Y. Zhao, "The influence of thermomechanical processing on microstructural evolution of Ti600 titanium alloy", Mat. Sci. Eng. A, Vol. 528, 2011, pp. 8410-8416.
[25] F. J. Humphreys and M. Hatherly, "Recrystallization and related annealing phenomena", Elsevier 2012, p. 251.
[26] A. H. Sheikhali, M. Morakabati and S. M. Abbasi, "Constitutive modeling for hot working behavior of SP-700 titanium alloy", J. Mat. Eng. Perf., Mat. Sci. Eng. A, Vol. 28, 2019, pp. 6525-6537.
[27] J. J. Jonas, C. Aranas, A. Fall and M. Jahazi, "Transformation Softening in Three Titanium Alloys", Mat. Des., Vol. 113, 2017, pp. 305- 310.
[28] K. Q. Lv, W. H. Cai, Z. Li, Z. Sh. Nong, L. Zhang, "Study on the Microstructure and Mechanical Properties of Dynamic Recrystallization of Metastable β Titanium Alloy", Materials Science Forum, Vol. 1064, 2022, pp. 177-182.
[29] A Esmaeilpour, HR Abedi, A Mirzaei, A Habibiyan, "Constructing the high temperature efficiency and instability maps of selective laser melted 316L stainless steel through artificial neural network modeling", J. Mat. Res. Tech., 2022, Vol. 18, pp. 4578-4589.
[30] P. Wanjara, M. Jahazi, H. Monajati and S. Yue, "Influence of thermomechanical processing on microstructural evolution in near-α alloy IMI834" Mat. Sci. Eng. A, Vol. 416, 2006, pp. 300-331.
[31] A. Momeni and S. M. Abbasi, "Effect of hot working on flow behavior of Ti-6Al-4V alloy in single phase and two phases regions", Mat. Des., Vol. 31, 2010, pp. 3599-3604.
[32] Y. V. R. K. Prasad, K. P. Rao and S. Sasidhar, "Hot working guide a compendium of processing maps", 2015, ASM international, p. 156.
[33] Y. P. Li, H. Matsumoto and A. Chiba, "Correcting the Stress-Strain Curve in the Stroke-Rate Controlling Forging Process" Metall. Mat. Trans. A, Vol. 40, 2009, pp. 1203-1211.