Synthesis of Single-Crystalline Octahedral Co3O4 with Solid-State Thermal Decomposition

الموضوعات :

Aliakbar Dehno Khalaji ¹

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تاريخ الإرسال : 29 الأربعاء , محرم, 1437 تاريخ التأكيد : 29 الأربعاء , محرم, 1437 تاريخ الإصدار : 10 الخميس , ربيع الأول, 1436

الکلمات المفتاحية:

ملخص المقالة :

In this paper, single crystalline octahedral Co3O4with dimensions about 100–500 nm and smooth surface has been prepared by solid-state thermal decomposition of cobalt(II) Schiff base complex Co((3,4-MeO-ba)2en)Cl2as new precursor at 450ºC under air atmosphere for 3.5 h. Surface morphology of the products were characterized by Fourier transform infrared spectroscopy (FT-IR), X-ray powder diffraction (XRD) and scanning electron microscopy (SEM).