Synthesis structural and anti-microbial characterization of nanostructured doped tin oxide

الموضوعات : Journal of Theoretical and Applied Physics

Achyutmohan Chaudhury ¹ , Utsa Debnath ² , Sujay Munshi ³ , Goutam Basak ⁴ , Avigyan Dutta ⁵ , Suvadip Masanta ⁶ , Achintya Singha ⁷ , Aritra Banerjee ⁸ , Debtanu Ghosh ⁹ , Partha Chatterjee ¹⁰ , Apurba Kanti Deb ¹¹

1 - Department of Chemistry Raiganj University, Raiganj, Uttar Dinajpur – 733134, West Bengal, India
2 - Department of Chemistry Raiganj University, Raiganj, Uttar Dinajpur – 733134, West Bengal, India
3 - Department of Physics Raiganj University, Raiganj, Uttar Dinajpur – 733134, West Bengal, India
4 - Department of Microbiology Raiganj University, Raiganj, Uttar Dinajpur – 733134, West Bengal, India
5 - Department of Physics University of Burdwan, Burdwan 713104, West Bengal, India
6 - Department of Physics, Main Campus Bose Institute, 93/1, Acharya Prafulla Chandra Road, Kolkata 700009, India
7 - Department of Physics, Main Campus Bose Institute, 93/1, Acharya Prafulla Chandra Road, Kolkata 700009, India
8 - Department of Physics University of Calcutta, 92 Acharya Prafulla Chandra Road, Kolkata-700 009, India
9 - Department of Physics Vivekananda Mahavidyalaya, Haripal, Hooghly 712405, India
10 - Department of Physics Vivekananda Mahavidyalaya, Haripal, Hooghly 712405, India
11 - Department of Physics, Raiganj University

تاريخ الإرسال : 06 الجمعة , جمادى الأولى, 1443 تاريخ التأكيد : 13 الأحد , جمادى الثانية, 1443 تاريخ الإصدار : 28 الثلاثاء , رجب, 1443

الکلمات المفتاحية: Rietveldanalysis, Nanocrystalline doped SnO2, Anti-microbial activity, X-ray powder diffraction, Raman and Fourier transform infrared Spectroscopy,

ملخص المقالة :

Nanocrystalline boron doped tin oxide and boron and silver co-doped SnO2 was successfully prepared by using simple sol-gel method. The structural property of as-prepared nanocrystalline materials was investigated by using X-ray powder diffraction, Raman spectroscopy, Fourier transform infrared spectroscopy and scanning electron microscopy. The infrared spectra of the prepared samples showed an incorporation of B and Ag in the SnO2 nanocrystals. The X-ray powder diffraction pattern of the as prepared sample demonstrated the formation of a rutile structure of SnO2 nanocrystallites with particle size of 35 nm and 98 nm for boron doped and co-doped samples respectively. The two different Sn-O bond distances are found to be varying in a different manner for the doped samples unlike pristine samples. A significant lattice microstrain was observed for co-doped samples indicating local lattice distortion. The prepared samples showed significant anti-microbial activities against some Gram-Positive & Gram-Negative bacteria in both water and DMSO medium. The prepared materials can be effective for water remediation.