Applicability of phenylpiperazine dithiocarbamate in the determination of As(III) in natural water and biological samples by differential pulse anodic stripping voltammetry
الموضوعات : Journal of the Iranian Chemical Research
Neelam Sreedhar
1
(Electroanalytical lab, Department of Chemistry, S.V.University, Tirupati, A.P., India)
Puthalapattu Prasad
2
(Electroanalytical lab, Department of Chemistry, S.V.University, Tirupati, A.P., India)
الکلمات المفتاحية: DPASV, As(III), Phenylpiperazine dithiocarbamate, Water and biological samples,
ملخص المقالة :
An efficient protocol for the selective oxidation of primary alcohols to aldehydes withH5IO6/V2O5 in ionic liquid [bmpy][PF6] has been developed. High yields of the products, mildreaction conditions and simple experimental procedure make this protocol complementary tothe existing methods. The catalyst can be reused for several times without obvious loss of thecatalytic activity.
[1] S. Venkatesan, A.S. Kumar, J.M. Zen, J. Mol. Catal. A 250 (2006) 87-93.
X. Liu & et al. / J. Iran. Chem. Res. 4 (2011) 135-139
139
[2] A.V. Biradar, M.K. Dongare, S.B. Umbarkar, Tetrahedron Lett. 50 (2009) 2885-2888.
[3] G. Bianchini, M. Crucianelli, F. de Angelis, V. Neri, R. Saladino, Tetrahedron Lett. 46 (2005) 2427-
2432.
[4] F.M. Menger, C. Lee, Tetrahedron Lett. 22 (1981) 1655-1656.
[5] C.K. Lee, B.S. Koo, Y.S. Lee, H. Cho, K.K. Lee, J. Bull. Korean Chem. Soc. 23 (2002) 1667-1670.
[6] R.A. Strecker, N.J. Randolph, US Pat. (1982) 4338442.
[7] K.R. Seddon, A. Stark, Green Chem. 4 (2002) 119-123.
[8] A. Wolfson, S. Wuyts, V.D. De, I.F.J. Vankelecom, P.A. Jacobs, Tetrahedron Lett. 43 (2002) 8107-
8110.
[9] B.S. Chhikara, S. Tehlan, A. Kumar, Synlett. (2005) 63-65.
[10] A. Kumar, N. Jain, S.M. Chauhan, Synlett. (2007) 411-414.
[11] N. Jiang, A.J. Ragauskas, J. Org. Chem. 71 (2006) 7087-7090.
[12] S.E. Martin, D.F. Suarez, Tetrahedron Lett. 43 (2002) 4475-4479.
[13] M. Saravanababu, J.L. Robert, Curr. Org. Synth. 2 (2005) 437-451.
[14] M.A.P. Martins, C.P. Frizzo, D.N. Moreira, N. Zanatta, H.G. Bonacorso, Chem. Rev. 108 (2008)
2015-2050.
[15] J. Muzart. Adv. Synth. Catal. 348 (2006) 275-295
[16] Y.L. Hu, X. Liu, M. Lu, H. Jiang. J. Chin. Chem. Soc. 57 (2010) 28-33.
[17] A. Butler, M.J. Clague, G.E. Meister, Chem. Rev. 94 (1994) 625-638.