MCM-41 functionalized sulfonic acid catalyzed one-pot synthesis of 1,8- dioxo-octahydroxanthenes
Subject Areas : Journal of the Iranian Chemical ResearchGholam Hossein Mahdavinia 1 , Mohammad Mehdi Ghanbari 2 , Hamid Sepehrian 3 , Fatemeh Kooti 4
1 - Islamic Azad University, Marvdasht Branch, Department of Chemistry, Marvdasht, Iran.
2 - Islamic Azad University, Sarvestan Branch, Department of Chemistry, Fars, Iran.
3 - Nuclear Science and Technology Research Institute, AEOI, P.O. Box 11365/8486, Tehran, Iran
4 - Faculty of Chemistry, Teacher Training University, 49 Mofateh St., Tehran, Iran.
Keywords: One-pot, MCM-41-R-SO3H, Heterogeneous, Hydroxanthene, Multicomponent,
Abstract :
MCM-41-R-SO3H catalyzed one-pot synthesis of 1,8-dioxo-octahydroxanthenes is reportedunder reflux conditions. The catalyst is easily prepared, highly stable, very simple to handle andrecycled for five times without loss of significant activity
[1] C.T. Kresge, M.E. Leonowicz, W.J. Roth, J.C. Vartuli, J.S. Beck, Nature 359 (1992) 710-712.
[2] W. Zhang, T.R. Pauly, T.J. Pinnavaia, Chem. Mater. 9 (1997) 2491-2498.
[3] A. Galarneau, D. Desplantier-Giscard, F. Di Renzo, F. Fajula, Catal. Today 68 (2001) 191-200.
[4] (a) W.M. Van Rhijn, D.E. De Vos, B.F. Sels, W.D. Bossaert, P.A. Jacobs, Chem. Commun. (1998)
317-318; (b) D. Das, J.F. Lee, S. Cheng, Chem. Commun. (2001) 2178-2179; (c) B. Karimi, D.
Zareyee, Tetrahedron Lett. 46 (2005) 4661-4665; (d) D. Zareyee, B. Karimi, Tetrahedron Lett.
48(2007) 1277-1280; (e) G.H. Mahdavinia, H. Sepehrain, Chin. Chem. Lett, 19 (2008) 1435-1439.
[5] J.P. Poupelin, G. Saint-Rut, O. Foussard-Blanpin, G. Narcisse, G. Uchida- Ernouf, R. Lacroix, Eur. J.
Med. Chem.13 (1978) 67-71.
[6] R.M .Ion, A .Planner, K .Wiktorowicz, D. Frackowiak, Acta Biochim. Pol. 45(1998) 833-845.
[7] R.J. Sarma, J.B. Baruah, Dyes Pigm. 64 (2005) 91-92.
[8] T.S. Jin, J.S. Zhang, J.C. Xiao, A.Q. Wang, T.S. Li, Synlett (2004) 866-870.
[9] X.-S. Wang, D.-Q. Shi, Y.-L. Li, H. Chen, X.-Y. Wei, Z.-M. Zong, Synth. Commun. 35 (2005) 97-
104.
[10] F. Darvish, S. Balalaei, F. Chadegani, P. Salehi, Synth. Commun. 37 (2007) 1059-1067.
[11] T-S. Jin, J-S. Zhang, A-Q. Wang, T-S. Li, Ultrason. Sonochem.13 (2006) 220-224.