Preparation of (MWCNTs)-COOH/CeO2Hybrid as an Efficient Catalyst for Claisen-Schmidt Condensation

Subject Areas : Polymer

Tahereh Heidarzadeh ¹ , Navabeh Nami ² , Daryoush Zareyee ³

1 - Department of Chemistry, Qaemshahr Branch, Islamic Azad University, Qaemshahr, Iran
2 - Department of Chemistry, Qaemshahr Branch, Islamic Azad University, Qaemshahr, Iran
3 - Department of Chemistry, Qaemshahr Branch, Islamic Azad University, Qaemshahr, Iran

Received: 2021-05-19 Accepted : 2021-05-19 Published : 2021-07-01

Keywords:

Abstract :

Acid functionalized multi-walled carbon nanotubes/CeO2 (MWCNTs)-COOH/CeO2 hybrid was fabricated by the reaction of functionalized (MWCNTs)-COOH and Ce(NO3)2.6H2O in acetic acid. Synthesis of CeO2 nanoparticles and their conjugation on the surface of (MWCNTs)-COOH have been confirmed by FT-IR, scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), and Energy-dispersive X-ray spectroscopy (EDX). The modification of MWCNTs-COOH with CeO2 produced an efficient catalyst for the Claisen–Schmidt condensation, soa large variety of chalconeswere obtained in high yield using a catalytic amount of (MWCNTs)-COOH/CeO2 hybrid (5 mol%).

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